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Laboratory

Anasori Lab Facilities 

The Anasori lab focuses on the fundamental understanding of the synthesis of novel layered nanostructures (MAX, MXenes, etc.) and investigating their mechanical, high-temperature, electronic and electrochemical behaviors and properties.

 

The members of the Anasori lab group have access to the following facilities :

Thermal Technology LLC

Specifications:

Maximum temperature: 2400 degrees Celsius

Force: 100 kN

Vacuum: 0.001 Torr

Operating pressure: Vacuum to 1 psi

Inert gases: Nitrogen/Argon/Helium

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Spark Plasma Sintering

Furnaces

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Tube Furnace-I

Carbolite Gero 1700

Specifications:

Maximum temperature: 1700 degrees Celsius

Heating zone: 30 cm

Tube length: 111.5 cm

Tube diameter: 6 cm

Tube Furnace-II

MTI Corporation GSL-1700X Series

Specifications:

Maximum temperature: 1700 degrees Celsius

Heating zone: 15 cm

Tube length: 100 cm

Tube diameter: 7.2 cm

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Box Furnace

MTI Corporation KSL-1200X 

Specifications:

Maximum temperature: 1200 degrees Celsius

Chamber dimensions: 30 x 20 x 12 cm

Capacity: 7.2 L

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Hydraulic Hot-Press 

Carver Inc.

Specifications:

Maximum temperature: 340 degrees Celsius

Pressure: 401 bar

Platen: 152 x 152 mm

Ram stroke: 152 mm

Fumehoods

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Specifications:

Work surface dimensions: 60 x 48 x 27 inches

Vertical sash equipped with provision for air, inert gas, and vacuum supply lines

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Glovebox

Vacuum Technology Inc

Specifications:

Chamber dimensions: 122 x 75 x 90 cm

Large antechamber: diameter 36 cm, length 60 cm

Small antechamber: diameter 15 cm, length 30 cm

Dust filter: HEPA 0.3 micron

Purifier: oxygen and moisture (less than 1 ppm)

Electrochemical Workstation

M204 AUTOLAB Metrohm

Specifications:

Potential range: +/- 10 V

Maximum current: +/- 400 mA

Compliance voltage: +/- 20 V

FRA32M impedance module

Dual-mode bipotentiostat

Rotating ring disk electrode with 150-300 mL cell

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Probe Sonicator

Fisherbrand-705 Sonic Dismembrator

Specifications:

Maximum power: 700 W

Pulse mode: 1 second to 24 hours

Programmable time: 1 second to 96 hours

Tip: microtip and replaceable horn tip

Processable volume: 20 to 250 mL

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High Energy Ball Milling

Retsch PM 100

Specifications:

Speed: 100 to 650 RPM

Grinding station: one

Grinding jar sizes: 25 mL and 50 mL

Grinding mode: dry and wet

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Jar Milling

Shimpo PTA-02 Jar Mill

Specifications:

Jar capacity: 10 L

Speed: 60 RPM

Number of jar: one

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Rotary Mixer

Fisherbrand Multi-Purpose Tube Rotators

Specifications:

Speed range: 5 to 80 RPM

Tube capacity: 50 mL

Timer range: 0 minutes to 99.59 hours

Centrifuges

Thermo Scientific SORVALL Legend X1

Specifications:

Rotor type: fixed angle

Rotor model: F15-8 x 50cy

Speed: 14000 RPM

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Centrifuge-I

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Centrifuge-II

Eppendorf 5804 R

Specifications:

Rotor type: swing bucket

Rotor model: S 4-72

Speed: 4200 RPM

Four-Probe Station 

Keithley 2000 with Four-Probe Station

Specifications:

13 built-in measurement functions

DC voltage: 100 nV to 1 kV

DC resistance: 100 micro ohms to 100 mega ohms

Equipped with SR-4 four-point prober

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Analytical Weighing Balance

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Weighing Balance-I

WANT Electronic Balance

Capacity: 200 g

Readability: 0.1 mg

Stabilization time: 4 seconds

Display: 2 line LCD with backlight

Weighing Balance-II

OHAUS PX224 with 80253384 Density Measurement Kit

Specifications:

Capacity: 220 g

Readability: 0.1 mg

Stabilization time: 4 seconds

Display: 2 line LCD with backlight

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Drill Press

WEN 4208 8-Inch 5- Speed Drill Press

Specifications:

Speed: 740/1100/1530/2100/3140 RPM

6.5 inch adjustable work table

Spindle travel: 2 inch

Chuck capacity: 0.5 inch

Bath Sonicator

Cole Palmer 8851

Specifications:

Capacity: 9.5 L

Frequency output: 42 kHz

Ultrasonic cleaner with timer, and heater

Temperature monitor, and degas

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Vacuum Ovens

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Specifications:

Maximum temperature: 200 degrees Celsius

LED digital PID controller

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Sample Storage Freezer

Kenmore Elite Upright Freezer

Specifications:

Minimum temperature: -20 degrees Celsius

Capacity: 660 L

X-ray Diffractogram with Hot-Stage
Available at the Integrated Nanosystems Development Institute (INDI) 

Bruker D8 Discover

Specifications:

Turbo X-ray source (TXS) with Cu anode

Focal brightness: 6 kW/square millimeter

LYNXEYE XE detector for 0D and 1D detection modes

VANTEC detector for 2D detection mode

Hot-stage: Anton Paar DHS 1100

Specifications:

Temperature range: 25 to 1100 degrees Celsius

Environment: inert/vacuum/air

Hot-stage: Anton Paar HTK2000N

(coming soon in 2023)

Specifications:

Temperature range: 25 to 2300 degrees Celsius

Environment: inert/vacuum/air

Location: Innovation Hall IO108

Integrated Nanosystems Development Institute (INDI)

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Field Emission Scanning Electron Microscope
Available at the Integrated Nanosystems Development Institute (INDI) 

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JEOL JSM-7800F 

Specifications:

Field emission gun

500 V to 30 kV

Resolution: 0.5 nm at 1 kV

Upto 500 nA beam current

Equipped with EDAX from AMTEK

Location: Innovation Hall IO108

Integrated Nanosystems Development Institute (INDI)

Atomic Force Microscope
Available at the Integrated Nanosystems Development Institute (INDI) 

Bruker Dimension IconIR

Specifications:

Powered by NanoScope 6 AFM controller

Tapping and contact mode

High performance nano-IR spectroscopy

Correlated chemical imaging

Location: Innovation Hall IO108

Integrated Nanosystems Development Institute (INDI)

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